N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone

Base Information

• Chemical Name: N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone
• CAS No.: 92030-03-0
• Molecular Formula: C₁₃H₁₃NO₆
• Molecular Weight: 279.249

Synonyms:N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone

Chemical Property of N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone

Chemical Property:

Purity/Quality:

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Technology Process of N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone

There total 6 articles about N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-benzyloxycarbonyl-γ-hydroxyglutamic acid (92076-00-1) → N-benzyloxycarbonyl-γ-hydroxyglutamic acid lactone (92030-03-0)

Guidance literature:

With hydrogenchloride; Heating;

DOI:10.1021/jo0514772

Reference yield:

→ (+/-)-erythro-N-benzyloxycarbonyl-4-hydroxy-glutamic acid-1-lactone (92030-03-0)

Guidance literature:

With toluene; unter Entfernen des entstehenden Wassers;

DOI:10.1021/ja01580a023

Reference yield:

lactone of threo-4-oxy-D,L-glutamic acid (67359-80-2,92619-77-7,150576-56-0,723233-77-0) → (+/-)-threo-N-benzyloxycarbonyl-4-hydroxy-glutamic acid-1-lactone (92030-03-0)

Guidance literature:

With sodium hydrogencarbonate;

DOI:10.1021/ja01580a023

upstream raw materials:

lactone of threo-4-oxy-D,L-glutamic acid

N-benzyloxycarbonyl-γ-hydroxyglutamic acid

4-acetoxy-2-acetylamino-2-ethoxycarbonyl-pentanedioic acid diethyl ester

2-amino-4-hydroxypentanedioic acid

Downstream raw materials:

4-benzyloxycarbonylamino-2-hydroxy-4-(4-methoxy-benzylcarbamoyl)-butyric acid

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