5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C₆₀-I_h)[5,6]fullerene-3''-carboxylate

Base Information

• Chemical Name: 5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C₆₀-I_h)[5,6]fullerene-3''-carboxylate
• CAS No.: 876144-93-3
• Molecular Formula: C₈₇H₂₁NO₆
• Molecular Weight: 1176.13

Synonyms:5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C₆₀-I_h)[5,6]fullerene-3''-carboxylate

Chemical Property of 5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C₆₀-I_h)[5,6]fullerene-3''-carboxylate

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Technology Process of 5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C₆₀-I_h)[5,6]fullerene-3''-carboxylate

There total 2 articles about 5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C₆₀-I_h)[5,6]fullerene-3''-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

61-{3'-[N-(diphenylmethylidene)aminoacetoxy]methyl}benzyl-61-methyl-61H-cyclopropa(C60-Ih)[5,6]fullerene-61,61-dicarboxylate → 5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C60-Ih)[5,6]fullerene-3''-carboxylate (876144-93-3)

Guidance literature:

With carbon tetrabromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200500694

Reference yield: 30.0%

3'-[methoxycarbonyl(acetoxymethyl)]phenyl-1'-methyl-N-(diphenylmethylideneamino) glycinate (876144-92-2) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → C72H12O5 + 5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C60-Ih)[5,6]fullerene-3''-carboxylate (876144-93-3)

Guidance literature:

With carbon tetrabromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 18h;

DOI:10.1002/ejoc.200500694

Reference yield: 50.0%

5',5'-diphenyl-3''-methyl-2',3'-(oxooxymethano[1,4]benzenomethanooxyoxo)-pyrrolo[3',4':1,9]-3''H-cyclopropa[16:17](C60-Ih)[5,6]fullerene-3''-carboxylate (876144-93-3) → C87H25NO6 + 15'-N-(diphenylmethyl)amino-3'-methyl-40H-3,21-(oxooxymethano[1,4]benzenomethanooxyoxomethano)-3'H-cyclopropa[1,9](C60-Ih)fullerene-3'-carboxylate

Guidance literature:

With boron trifluoride diethyl etherate; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; for 18h;

DOI:10.1002/ejoc.200500694

upstream raw materials:

3'-[methoxycarbonyl(acetoxymethyl)]phenyl-1'-methyl-N-(diphenylmethylideneamino) glycinate

fullerene-C₆₀

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