Technology Process of C18H17NO2
There total 4 articles about C18H17NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
acetonitrile;
at 0 - 20 ℃;
for 5h;
DOI:10.1055/s-0030-1259703
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; N,N-dimethylglycine hydrochoride; caesium carbonate / 1,4-dioxane / 4.5 h / Inert atmosphere; Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / acetonitrile / 5 h / 0 - 20 °C
With
copper(l) iodide; N,N-dimethylglycine hydrochoride; sodium hydride; caesium carbonate; toluene-4-sulfonic acid;
In
1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0030-1259703
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; N,N-dimethylglycine hydrochoride; caesium carbonate / 1,4-dioxane / 4.5 h / Inert atmosphere; Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / acetonitrile / 5 h / 0 - 20 °C
With
copper(l) iodide; N,N-dimethylglycine hydrochoride; sodium hydride; caesium carbonate; toluene-4-sulfonic acid;
In
1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0030-1259703
