Technology Process of C30H29NO8
There total 3 articles about C30H29NO8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; potassium carbonate;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 3h;
DOI:10.1002/anie.200704577
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
2.1: sodium hydroxide / water / 0.25 h / 20 °C / Inert atmosphere
2.2: 0 °C / pH 1 / Inert atmosphere
2.3: 0.5 h / 80 °C / Inert atmosphere
3.1: caesium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere
With
boron tribromide; tetra-(n-butyl)ammonium iodide; caesium carbonate; sodium hydroxide;
In
dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide / water / 0.25 h / 20 °C / Inert atmosphere
1.2: 0 °C / pH 1 / Inert atmosphere
1.3: 0.5 h / 80 °C / Inert atmosphere
2.1: caesium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere
With
tetra-(n-butyl)ammonium iodide; caesium carbonate; sodium hydroxide;
In
water; N,N-dimethyl-formamide;