2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

Base Information

Chemical Name:2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile
CAS No.:850312-47-9
Molecular Formula:C₁₉H₂₀N₄O
Molecular Weight:320.394
Hs Code.:

Synonyms:2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

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Technology Process of 2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

There total 4 articles about 2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2-amino-3-([4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylidene]amino)but-2-enedinitrile

: 850312-47-9
2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 2h;
DOI:10.1021/jo047792q

Reference yield:

: 850222-68-3
4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzaldehyde

: 850312-47-9
2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / ethanol / 20 h / Heating

2: 96 percent / NaBH₄ / tetrahydrofuran; methanol / 2 h

With sodium tetrahydroborate; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jo047792q

Reference yield:

: 50626-34-1,108266-85-9,108266-86-0
bicyclo[2.2.1]hept-5-en-2-ylmethyl 4-methylbenzenesulfonate

: 850312-47-9
2-amino-3-[4-(bicyclo[2.2.1]hept-5-en-2-ylmethoxy)benzylamino]but-2-enedinitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Cs₂CO₃ / dimethylformamide / 16 h / 100 °C

2: 73 percent / ethanol / 20 h / Heating

3: 96 percent / NaBH₄ / tetrahydrofuran; methanol / 2 h

With sodium tetrahydroborate; caesium carbonate; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo047792q