10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

Base Information

Chemical Name:10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile
CAS No.:1266610-85-8
Molecular Formula:C₂₀H₁₈N₂O₂S
Molecular Weight:350.441
Hs Code.:

Synonyms:10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

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Technology Process of 10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

There total 4 articles about 10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1266610-56-3
C₂₁H₂₀ClIN₂O₃S

: 1266610-85-8
10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

Guidance literature:: With copper diacetate; caesium carbonate; In N,N-dimethyl-formamide; at 125 ℃; for 3h;
DOI:10.1002/chem.201002628

Reference yield:

: 68819-94-3
p-tolyl benzeneselenosulfonate

: 1266610-85-8
10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloroform / 2.5 h / Irradiation

1.2: 3.42 h / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide; water / 16 h / 20 °C

3.1: caesium carbonate; copper diacetate / N,N-dimethyl-formamide / 3 h / 125 °C

With copper diacetate; potassium carbonate; caesium carbonate; In chloroform; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201202307

Reference yield:

: 1266610-54-1
1-(5-chlorohex-1-ynylsulfonyl)-4-methylbenzene

: 1266610-85-8
10-(p-toluenesulfonyl)-6,7,8,9-tetrahydropyrido[1,2-a]indole-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide; water / 16 h / 20 °C

2: caesium carbonate; copper diacetate / N,N-dimethyl-formamide / 3 h / 125 °C

With copper diacetate; potassium carbonate; caesium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201202307