9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Base Information

Chemical Name:9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene
CAS No.:122949-74-0
Molecular Formula:C₂₈H₂₈O₃Si
Molecular Weight:440.614
Hs Code.:

Synonyms:9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Suppliers and Price of 9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

There total 3 articles about 9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 122949-72-8
9,10-dihydro-9,10-dimethoxy-11-oxo-12-(phenylethynyl)-12-(trimethylsiloxy)-9,10-ethanoanthracene

: 122949-74-0
9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Guidance literature:: With 5-decyne; In tetrahydrofuran; for 7h; Ambient temperature; Irradiation;
DOI:10.1021/jo00284a015

Reference yield:

: 122949-71-7
9,10-dihydro-9,10-dimethoxy-9,10-ethanoanthracene-11,12-dione

: 122949-74-0
9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Guidance literature:: Multi-step reaction with 2 steps

2: 68 percent / 5-decyne / tetrahydrofuran / 7 h / Ambient temperature; Irradiation

With 5-decyne; In tetrahydrofuran;
DOI:10.1021/jo00284a015

Reference yield:

: 122949-70-6
4a,9a-dichloro-4,9-dimethoxy-2-oxo-4,4a,9,9a-tetrahydro-4,9-<1',2'>benzenonaphtho<2,3-d>-1,3-dioxole

: 122949-74-0
9,10-dihydro-9,10-dimethoxy-11-(phenylethynyl)11-(trimethylsiloxy)-9,10-methanoanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: aq. 10percent HCl / tetrahydrofuran / 25 h / Ambient temperature

3: 68 percent / 5-decyne / tetrahydrofuran / 7 h / Ambient temperature; Irradiation

With hydrogenchloride; 5-decyne; In tetrahydrofuran;
DOI:10.1021/jo00284a015