H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

Base Information

Chemical Name:H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph
CAS No.:138775-40-3
Molecular Formula:C₃₂H₄₄N₄O₆
Molecular Weight:580.725
Hs Code.:

H-L-(N<sup>δ</sup>-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

Synonyms:H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

Chemical Property:

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Technology Process of H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

There total 8 articles about H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138775-39-0
Fmoc-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

: 138775-40-3
H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

Guidance literature:: With diethylamine; In acetonitrile; Ambient temperature;
DOI:10.1021/jm00099a019

Reference yield:

: 109425-55-0,118476-89-4
Fmoc-Orn(Boc)-OH

: 138775-40-3
H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N,N-diisopropylethylamine (DIEA), bis(2-oxo-3-oxazolidinyl)phosphinic chloride (BOP-Cl), 2.) N,N-diisopropylethylamine (DIEA) / 1.) CH₂Cl₂, 1.5 h, 2.) CH₂Cl₂, 0 deg C, 16 h

2: diethylamine / acetonitrile / Ambient temperature

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; diethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1021/jm00099a019

Reference yield:

: H-D-(N-Me)Phe-L-Pro-OCH₂Ph hydrochloride

: 138775-40-3
H-L-(N^δ-Boc)Orn-D-(N-Me)Phe-L-Pro-OCH2Ph

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N,N-diisopropylethylamine (DIEA), bis(2-oxo-3-oxazolidinyl)phosphinic chloride (BOP-Cl), 2.) N,N-diisopropylethylamine (DIEA) / 1.) CH₂Cl₂, 1.5 h, 2.) CH₂Cl₂, 0 deg C, 16 h

2: diethylamine / acetonitrile / Ambient temperature

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; diethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1021/jm00099a019