<2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid

Base Information

• Chemical Name: <2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid
• CAS No.: 97513-13-8
• Molecular Formula: C₃₁H₃₂N₆O₂P₂
• Molecular Weight: 582.582
• Mol file: 97513-13-8.mol

Synonyms:<2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid

Chemical Property of <2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of <2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid

There total 1 articles about <2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

Bis(N,N,N',N'-tetramethylformamidinium)ether-bis(trifluormethansulfonat) (78581-29-0) + diphenylphosphorylazide (5353-66-2) → <2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid (97513-13-8) + tetramethylurea (632-22-4)

Guidance literature:

In acetonitrile; -20 deg C to r.t. 30 min;

Reference yield: 81.0%

<2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid (97513-13-8) → 3,4-Bis(dimethylamino)-5-(diphenylphosphoryl)-1H-pyrazol (97513-18-3)

Guidance literature:

In acetonitrile; for 9h; Ambient temperature; further conditions: 170 deg C, 3 h, 1,2-dichlorobenzene; photolysis, 3 h, benzene;

Reference yield: 65.0%

<2-<2,2-Bis(dimethylamino)-1-(diphenylphosphoryl)vinyl>-2H-tetrazol-5-yl>diphenylphosphanoxid (97513-13-8) → 4,5-Bis(dimethylamino)-1,3-bis(diphenylphosphoryl)-1H-pyrazol (97513-16-1)

Guidance literature:

In 1,3,5-trimethyl-benzene; at 140 ℃; for 3h;

upstream raw materials:

Bis(N,N,N',N'-tetramethylformamidinium)ether-bis(trifluormethansulfonat)

diphenylphosphorylazide

Downstream raw materials:

3,4-Bis(dimethylamino)-5-(diphenylphosphoryl)-1H-pyrazol

4,5-Bis(dimethylamino)-1,3-bis(diphenylphosphoryl)-1H-pyrazol