C₄₉H₆₅N₇OSi₂

Base Information

Chemical Name:C₄₉H₆₅N₇OSi₂
CAS No.:1609377-78-7
Molecular Formula:C₄₉H₆₅N₇OSi₂
Molecular Weight:824.272
Hs Code.:

C<sub>49</sub>H<sub>65</sub>N<sub>7</sub>OSi<sub>2</sub>

Synonyms:C₄₉H₆₅N₇OSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₆₅N₇OSi₂

Chemical Property:

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Technology Process of C₄₉H₆₅N₇OSi₂

There total 4 articles about C₄₉H₆₅N₇OSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1609377-77-6
C₃₉H₄₇I₂N₇O

: 1066-54-2
trimethylsilylacetylene

: 1609377-78-7
C₄₉H₆₅N₇OSi₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201304161

Reference yield:

: 162993-50-2
3,5-diazido-benzoic acid

: 1609377-78-7
C₄₉H₆₅N₇OSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 15 h / 20 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate / toluene; water; ethanol / 12 h / 20 °C / Inert atmosphere

3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1002/chem.201304161

Reference yield:

: 1609377-76-5
C₂₃H₃₇N₇O

: 1609377-78-7
C₄₉H₆₅N₇OSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate / toluene; water; ethanol / 12 h / 20 °C / Inert atmosphere

2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1002/chem.201304161