H₄Os₆(CO)15(S)2(HCNC₆H₅)2

Base Information

Chemical Name:H₄Os₆(CO)15(S)2(HCNC₆H₅)2
CAS No.:83746-83-2
Molecular Formula:C₂₉H₁₆N₂O₁₅Os₆S₂
Molecular Weight:1837.78
Hs Code.:

H<sub>4</sub>Os<sub>6</sub>(CO)15(S)2(HCNC<sub>6</sub>H<sub>5</sub>)2

Synonyms:H₄Os₆(CO)15(S)2(HCNC₆H₅)2

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Chemical Property of H₄Os₆(CO)15(S)2(HCNC₆H₅)2

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Technology Process of H₄Os₆(CO)15(S)2(HCNC₆H₅)2

There total 1 articles about H₄Os₆(CO)15(S)2(HCNC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 80399-46-8
HOs₃(CO)9(S)(HCNC₆H₅)

: 83746-83-2
H₄Os₆(CO)15(S)2(HCNC₆H₅)2

: 83731-67-3
H₆Os₆(CO)14(S)2(HCNC₆H₅)2

: 83731-68-4
H₄Os₆(CO)15(S)2(HCNC₆H₅)2

Guidance literature:: With hydrogen; In octane; a soln. of Os3-cluster in octane was heated to reflux for 1.75 h while H2 was bubbled through the soln.; the solvent was removed in vacuo, residue chromd. on SiO2 plates with 4:1 hexane/CH2Cl2 as eluent;

Reference yield: 78.0%

: 83746-83-2
H₄Os₆(CO)15(S)2(HCNC₆H₅)2

: 80399-46-8
HOs₃(CO)9(S)(HCNC₆H₅)

Guidance literature:: With carbon monoxide; In octane; CO was bubbled through an octane soln. of Os-cluster that was heated toreflux; the solvent was removed in vacuo, residue chromd. on SiO2 plates with 5:1 hexane/CH2Cl2 as eluent;

Reference yield: 58.0%

: 83746-83-2
H₄Os₆(CO)15(S)2(HCNC₆H₅)2

: 83731-69-5
Os₆(CO)15(S)2(HCNC₆H₅)2

: 83731-68-4
H₄Os₆(CO)15(S)2(HCNC₆H₅)2

Guidance literature:: In octane; an octane soln. of Os-cluster was heated to reflux for 4.5 h while argon was bubbled through the soln.; the solvent was removed in vacuo, residue chromd. on SiO2 plates with 5:1 hexane/CH2Cl2 as eluent;