ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

Base Information

Chemical Name:ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate
CAS No.:172419-87-3
Molecular Formula:C₁₄H₁₈FNO₃
Molecular Weight:267.3
Hs Code.:

Synonyms:ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

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Chemical Property of ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

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Technology Process of ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

There total 1 articles about ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22116-33-2
2-(4-fluoro-benzyl-amino)-ethanol

: 172419-87-3
ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) potassium tert-butoxide / 1.) Et₂O, RT, 5 d, 2.) DME, a) RT, 2 h, b) reflux, 1 h

2: 98 percent / conc. H₂SO₄ / 20 h / Heating

With sulfuric acid; potassium tert-butylate;
DOI:10.1002/jlcr.2580361004

Reference yield: 98.0%

: 172419-87-3
ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

: 172419-88-4
<2-2H2>-4-(4-fluorobenzyl)-2-hydroxymethylmorpholine

Guidance literature:: With sodium borodeuteride; lithium chloride; In tetrahydrofuran; ethanol; for 15h; Ambient temperature;
DOI:10.1002/jlcr.2580361004

Reference yield:

: 172419-87-3
ethyl 4-(4-fluorobenzyl)-2-morpholinecarboxylate

: 172419-89-5
<2-2H2>-N-<<4-(4-fluorobenzyl)-2-morpholinyl>methyl>phthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / lithium chloride, sodium borodeuteride / tetrahydrofuran; ethanol / 15 h / Ambient temperature

2: 96 percent / triphenylphosphine, dimethyl azodicarboxylate / tetrahydrofuran / 15 h / Ambient temperature

With sodium borodeuteride; dimethyl azodicarboxylate; triphenylphosphine; lithium chloride; In tetrahydrofuran; ethanol;
DOI:10.1002/jlcr.2580361004