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Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester

Base Information Edit
  • Chemical Name:Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester
  • CAS No.:100311-73-7
  • Molecular Formula:C33H40O4Si
  • Molecular Weight:528.764
  • Hs Code.:
  • Mol file:100311-73-7.mol
Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester

Synonyms:Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester

Suppliers and Price of Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester Edit
Chemical Property:
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SDS file from LookChem

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Technology Process of Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester

There total 9 articles about Benzoic acid (Z)-(S)-9-(tert-butyl-diphenyl-silanyloxy)-10-oxo-dec-6-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 6 steps
1: lithium hexamethyldisilazane (LiHMDS) / tetrahydrofuran; hexamethylphosphoric acid triamide / 2.5 h / -78 - 20 °C
2: NaHCO3 / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / Ambient temperature
3: 68 percent / AlH3*Et2O / tetrahydrofuran / 0.5 h / 0 °C
4: 85 percent / Et3N / CH2Cl2 / 0 °C
5: aq. TFA / tetrahydrofuran / Ambient temperature
6: Na2CO3, Pb(OAc)4 / CH2Cl2 / 0.25 h / -78 °C
With lead(IV) acetate; aluminium hydride * diethyl ether; sodium hydrogencarbonate; sodium carbonate; triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/jo00356a004
Guidance literature:
Multi-step reaction with 3 steps
1: 85 percent / Et3N / CH2Cl2 / 0 °C
2: aq. TFA / tetrahydrofuran / Ambient temperature
3: Na2CO3, Pb(OAc)4 / CH2Cl2 / 0.25 h / -78 °C
With lead(IV) acetate; sodium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00356a004
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