Technology Process of C25H42O5SSi2
There total 8 articles about C25H42O5SSi2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate; ozone;
In
water; acetonitrile;
at 0 ℃;
for 3h;
Inert atmosphere;
DOI:10.1039/c2cc33054g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / methanol / 3 h / 0 °C / Inert atmosphere
2: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 8 h / Inert atmosphere
4: 3-chloro-benzenecarboperoxoic acid / 11 h / 0 °C / Inert atmosphere
5: 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate; ozone / water; acetonitrile / 3 h / 0 °C / Inert atmosphere
With
sodium tetrahydroborate; 1,1,1-trifluoro-2-propanone; trimethylsilyl trifluoromethanesulfonate; sodium hydrogencarbonate; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc33054g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 8 h / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / 11 h / 0 °C / Inert atmosphere
3: 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate; ozone / water; acetonitrile / 3 h / 0 °C / Inert atmosphere
With
1,1,1-trifluoro-2-propanone; trimethylsilyl trifluoromethanesulfonate; sodium hydrogencarbonate; ozone; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc33054g
