1--2-(p-nitrophenoxy)ethane

Base Information

• Chemical Name: 1--2-(p-nitrophenoxy)ethane
• CAS No.: 130745-32-3
• Molecular Formula: C₁₆H₁₈N₂O₄
• Molecular Weight: 302.33

Synonyms:1--2-(p-nitrophenoxy)ethane

Chemical Property of 1--2-(p-nitrophenoxy)ethane

Chemical Property:

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Technology Process of 1--2-(p-nitrophenoxy)ethane

There total 1 articles about 1--2-(p-nitrophenoxy)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

1-(2-bromoethoxy)-4-nitrobenzene (13288-06-7) + 3-Dimethylaminophenol (99-07-0) → 1--2-(p-nitrophenoxy)ethane (130745-32-3)

Guidance literature:

With potassium hydroxide; tetrabutylammomium bromide; In 2-methoxy-ethanol; at 100 ℃; for 2.5h;

DOI:10.1246/bcsj.68.3247

Reference yield:

1--2-(p-nitrophenoxy)ethane (130745-32-3) → Methyl-{3-[2-(4-nitroso-phenoxy)-ethoxy]-phenyl}-amine (130766-46-0) + Methyl-{3-[2-(4-nitro-phenoxy)-ethoxy]-phenyl}-amine (130745-39-0)

Guidance literature:

In benzene; Irradiation;

DOI:10.1246/cl.1990.1559

Reference yield:

1--2-(p-nitrophenoxy)ethane (130745-32-3) → Methyl-{3-[2-(4-nitroso-phenoxy)-ethoxy]-phenyl}-amine (130766-46-0) + Methyl-{3-[2-(4-nitro-phenoxy)-ethoxy]-phenyl}-amine (130745-39-0) + N-Methyl-N-{3-[2-(4-nitro-phenoxy)-ethoxy]-phenyl}-formamide (130745-40-3)

Guidance literature:

In benzene; Mechanism; Product distribution; Irradiation; rel. reactivity of homologs; magnetic field effects;

DOI:10.1246/cl.1990.1559

upstream raw materials:

1-(2-bromoethoxy)-4-nitrobenzene

3-Dimethylaminophenol

Downstream raw materials:

Methyl-{3-[2-(4-nitroso-phenoxy)-ethoxy]-phenyl}-amine

Methyl-{3-[2-(4-nitro-phenoxy)-ethoxy]-phenyl}-amine

N-Methyl-N-{3-[2-(4-nitro-phenoxy)-ethoxy]-phenyl}-formamide

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