1-phenyl-2-methyl-3-p-tolylcyclopropene

Base Information

Chemical Name:1-phenyl-2-methyl-3-p-tolylcyclopropene
CAS No.:96633-34-0
Molecular Formula:C₁₇H₁₆
Molecular Weight:220.314
Hs Code.:

Synonyms:1-phenyl-2-methyl-3-p-tolylcyclopropene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-2-methyl-3-p-tolylcyclopropene

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Technology Process of 1-phenyl-2-methyl-3-p-tolylcyclopropene

There total 2 articles about 1-phenyl-2-methyl-3-p-tolylcyclopropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 96633-33-9
3-phenyl-4-p-tolylbuten-2-one tosylhydrazone

: 96633-34-0
1-phenyl-2-methyl-3-p-tolylcyclopropene

Guidance literature:: With sodium hydride; tert-butyl alcohol; In hexane; diethylene glycol dimethyl ether; for 4h; Irradiation;
DOI:10.1021/jo00214a027

Reference yield:

: 38661-89-1
3-phenyl-4-p-tolylbuten-2-one

: 96633-34-0
1-phenyl-2-methyl-3-p-tolylcyclopropene

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / conc. HCl / methanol / 1 h / Heating

2: 49 percent / NaH, tert-butyl alcohol / hexane; bis-(2-methoxy-ethyl) ether / 4 h / Irradiation

With hydrogenchloride; sodium hydride; tert-butyl alcohol; In methanol; hexane; diethylene glycol dimethyl ether;
DOI:10.1021/jo00214a027