4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

Base Information

Chemical Name:4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate
CAS No.:153757-00-7
Molecular Formula:C₁₈H₁₉ClN₂O₅
Molecular Weight:378.812
Hs Code.:

Synonyms:4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

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Chemical Property of 4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

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Technology Process of 4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

There total 4 articles about 4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 153756-89-9
4-<(tert-butoxycarbonyl)amino>phenyl chloroformate

: 95-85-2
2-hydroxy-5-chloro-aniline

: 153757-00-7
4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

Guidance literature:: In diethyl ether; for 4h; Heating;
DOI:10.1021/jm00020a012

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 153757-00-7
4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / tetrahydrofuran / 24 h / Heating

2: 93 percent / N,N-dimethylaniline / ethyl acetate; toluene / 2 h / 0 - 5 °C

3: 85 percent / diethyl ether / 4 h / Heating

With N,N-dimethyl-aniline; In tetrahydrofuran; diethyl ether; ethyl acetate; toluene;
DOI:10.1021/jm00020a012

Reference yield:

: 54840-15-2
4-N-tert-butoxycarbonylaminophenol

: 153757-00-7
4-<(tert-butoxycarbonyl)amino>phenyl N-(5-chloro-2-hydroxyphenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / N,N-dimethylaniline / ethyl acetate; toluene / 2 h / 0 - 5 °C

2: 85 percent / diethyl ether / 4 h / Heating

With N,N-dimethyl-aniline; In diethyl ether; ethyl acetate; toluene;
DOI:10.1021/jm00020a012