methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

Base Information

Chemical Name:methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate
CAS No.:1445872-63-8
Molecular Formula:C₃₁H₃₀F₃NO₁₂
Molecular Weight:665.574
Hs Code.:

Synonyms:methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

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Chemical Property of methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

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Technology Process of methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

There total 1 articles about methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1269802-97-2
methyl 1-hydroxy-6-phenyl-4-(trifluoromethyl)-1H-indole-2-carboxylate

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1445872-63-8
methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

Guidance literature:: With potassium carbonate; In acetone; for 24h; Inert atmosphere;

Reference yield: 98.0%

: 1445872-63-8
methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

: 1445872-61-6
methyl 6-phenyl-1-(β-D-glucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

Guidance literature:: methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate; With methanol; sodium methylate; In methanol; at 0 - 20 ℃; for 3h; Inert atmosphere;

In methanol; pH=7;

Reference yield:

: 1445872-63-8
methyl 6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylate

: 1445872-62-7
6-phenyl-1-(β-D-2,3,4,6-tetra-O-acetylglucopyranosyl)oxy-4-(trifluoromethyl)-1H-indole-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate; methanol / methanol / 3 h / 0 - 20 °C / Inert atmosphere

1.2: acidic resin Amberlite? IR 120 H / pH 7

2.1: lithium hydroxide; water / methanol; tetrahydrofuran / Inert atmosphere

2.2: acidic resin Amberlite? IR 120 H / pH Ca. 2

3.1: pyridine / 24 h / 20 °C / Inert atmosphere

With pyridine; methanol; water; sodium methylate; lithium hydroxide; In tetrahydrofuran; methanol;