N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

Base Information

Chemical Name:N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine
CAS No.:1352561-46-6
Molecular Formula:C₃₆H₃₇NO₄
Molecular Weight:547.694
Hs Code.:

Synonyms:N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

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Chemical Property of N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

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Technology Process of N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

There total 4 articles about N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1-C-formyl-3,4,6-tri-O-benzyl-D-galactal

: 1352561-46-6
N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

Guidance literature:: In dichloromethane; for 2h; Molecular sieve;
DOI:10.1016/j.carres.2011.10.023

Reference yield:

: 1320325-00-5
1-cyano-3,4,6-tri-O-benzyl-D-galactal

: 1352561-46-6
N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; sodium hypophosphite; acetic acid / water / 3 h / 20 °C / Cooling with ice

2: dichloromethane / 2 h / Molecular sieve

With pyridine; sodium hypophosphite; acetic acid; In dichloromethane; water;
DOI:10.1016/j.carres.2011.10.023

Reference yield:

: 3737-59-5
2,6-anhydro-D-glycero-L-manno-heptononitrile

: 1352561-46-6
N-((S)-1-phenylethyl)-(3,4,6-tri-O-benzyl-2-deoxy-D-lyxo-hex-2-enopyranosyl)formaldimine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide

2: pyridine; sodium hypophosphite; acetic acid / water / 3 h / 20 °C / Cooling with ice

3: dichloromethane / 2 h / Molecular sieve

With pyridine; sodium hypophosphite; sodium hydride; acetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.10.023