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Technology Process of 3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)

3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)

Base Information
  • Chemical Name:3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)
  • CAS No.:75802-05-0
  • Molecular Formula:3C13H22N*C22O22PRh10
  • Molecular Weight:2253.23
  • Hs Code.:
3((C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>)N(C<sub>2</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*(Rh<sub>10</sub>P(CO)22)<sup>(3-)</sup>=((C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>)N(C<sub>2</sub>H<sub>5</sub>)3)3(Rh<sub>10</sub>P(CO)22)

Synonyms:3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)

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Chemical Property of 3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)
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Technology Process of 3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)

There total 1 articles about 3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.2%

acetylacetonatodicarbonylrhodium(l)

acetylacetonatodicarbonylrhodium(l)

N-benzyl-N,N,N-triethylammonium chloride
56-37-1

N-benzyl-N,N,N-triethylammonium chloride

3((C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>)N(C<sub>2</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*(Rh<sub>10</sub>P(CO)22)<sup>(3-)</sup>=((C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>)N(C<sub>2</sub>H<sub>5</sub>)3)3(Rh<sub>10</sub>P(CO)22)
75802-05-0

3((C6H5CH2)N(C2H5)3)(1+)*(Rh10P(CO)22)(3-)=((C6H5CH2)N(C2H5)3)3(Rh10P(CO)22)

Guidance literature:
With cesium benzoate; triphenylphosphine; cesium borohydride; In isopropyl alcohol; acetone; High Pressure; Rh(CO)2acac, PhCOOCs and PPh3 in CH3(OCH2CH2)4OCH3 mixed with CsBH4 in the same solvent, mixt. stirred for 12 h at 150-160°C under 6000 psi CO and H2, soln. filtered, toluene added, residue dissolved in acetone, (PhCH2NEt3)Cl in 2-propanol; ppt. filtered, washed with 2-propanol and vac. dried; elem. anal.;
DOI:10.1021/ic50215a047
upstream raw materials:

N-benzyl-N,N,N-triethylammonium chloride

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