2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid

Base Information

• Chemical Name: 2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid
• CAS No.: 82622-07-9
• Molecular Formula: C₂₇H₂₉NO₇
• Molecular Weight: 479.53

Synonyms:2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid

Chemical Property of 2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid

Chemical Property:

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Technology Process of 2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid

There total 1 articles about 2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(benzyloxy)-2,4-dimethoxy-3-methylbenzaldehyde (82622-02-4) + benzyl chloroformate (501-53-1,94274-21-2) + ethyl 2-cyanoacetate (105-56-6) → 2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid (82622-07-9)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/ja00382a042

Reference yield: 83.0%

(E)-2-Amino-1-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-4-phenyl-but-3-en-1-ol (82622-05-7,82622-06-8) + 2-Benzyloxycarbonylamino-3-(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-propionic acid (82622-07-9) → (2-(5-Benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-1-{(E)-1-[(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-hydroxy-methyl]-3-phenyl-allylcarbamoyl}-ethyl)-carbamic acid benzyl ester (82638-77-5)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;

DOI:10.1021/ja00382a042

upstream raw materials:

5-(benzyloxy)-2,4-dimethoxy-3-methylbenzaldehyde

benzyl chloroformate

ethyl 2-cyanoacetate

Downstream raw materials:

(2-(5-Benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-1-{(E)-1-[(5-benzyloxy-2,4-dimethoxy-3-methyl-phenyl)-hydroxy-methyl]-3-phenyl-allylcarbamoyl}-ethyl)-carbamic acid benzyl ester

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