1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

Base Information

Chemical Name:1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole
CAS No.:209958-68-9
Molecular Formula:C₂₈H₂₄F₃N₅O₃S
Molecular Weight:567.591
Hs Code.:

Synonyms:1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

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Chemical Property of 1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

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Technology Process of 1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

There total 5 articles about 1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 193006-34-7
4-(2'-tert-butylaminosulfonylphenyl)aniline

: N-(3-cyanophenyl)-3-trifluoromethyl-pyrazole-5-carboxylic acid chloride

: 209958-68-9
1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jm000409z

Reference yield:

: 367-57-7
1,1,1-Trifluoro-2,4-pentanedione

: 209958-68-9
1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 89.9 percent / aq. NaIO₄; RuCl₃*H₂O / acetonitrile / 18 h / 20 °C

2: oxalyl chloride; DMF / CH₂Cl₂ / 2 h / 20 °C

3: N,N-dimethylaminopyridine / CH₂Cl₂ / 24 h / 20 °C

With dmap; ruthenium trichloride; sodium periodate; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; acetonitrile;
DOI:10.1021/jm000409z

Reference yield:

: 27246-81-7
3-bromophenylhydrazine hydrochloride

: 209958-68-9
1-(3-cyanophenyl)-5-((2'-t-butylaminosulfonyl-[1,1']-biphen-4-yl)aminocarbonyl)-3-trifluoromethylpyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 89.9 percent / aq. NaIO₄; RuCl₃*H₂O / acetonitrile / 18 h / 20 °C

2: oxalyl chloride; DMF / CH₂Cl₂ / 2 h / 20 °C

3: N,N-dimethylaminopyridine / CH₂Cl₂ / 24 h / 20 °C

With dmap; ruthenium trichloride; sodium periodate; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; acetonitrile;
DOI:10.1021/jm000409z