ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

Base Information

Chemical Name:ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate
CAS No.:1453187-86-4
Molecular Formula:C₂₆H₂₈ClNO₃
Molecular Weight:437.966
Hs Code.:

Synonyms:ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

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Chemical Property of ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

Chemical Property:

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Technology Process of ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

There total 4 articles about ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(4-chlorophenyl)-2-(oct-1-yn-1-yl)benzamide

: 140-88-5,9003-32-1
ethyl acrylate

: 1453187-86-4
ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide; at 80 ℃; Temperature; Reagent/catalyst; Concentration;
DOI:10.1055/s-0033-1338873

Reference yield:

: 13421-13-1
4-chloro-2-iodobenzoic acid

: 1453187-86-4
ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / toluene

2: triethylamine / dichloromethane / 1 h

3: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 55 °C / Inert atmosphere

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 80 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide; toluene; 3: |Sonogashira Cross-Coupling;
DOI:10.1055/s-0033-1338873

Reference yield:

: 1377927-16-6
4-chloro-2-iodo-N-phenylbenzamide

: 1453187-86-4
ethyl (E)-3-[(Z)-1-(4-chlorophenylimino)-3-hexyl-1H-isochromen-4-yl]acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 55 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 80 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; 1: |Sonogashira Cross-Coupling;
DOI:10.1055/s-0033-1338873