trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate

Base Information

• Chemical Name: trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzo
• Molecular Formula: C₃₇H₃₀O₄
• Molecular Weight: 538.643

Synonyms:trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate

Chemical Property of trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzo

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

There total 1 articles about trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

trans-7,8-dihydroxy-1-isopropenyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate → trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate (107616-90-0)

Guidance literature:

With hydrogen; platinum on activated charcoal; In ethyl acetate; for 72h;

DOI:10.1021/jo00387a023

Reference yield:

trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate (107616-90-0) → Benzoic acid 1-isopropyl-9,10-dihydro-benzo[def]chrysen-8-yl ester (107616-91-1)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 24h; Heating;

DOI:10.1021/jo00387a023

Reference yield:

trans-7,8-dihydroxy-1-isopropyl-7,8,9,10-tetrahydrobenzopyrene dibenzoate (107616-90-0) → Benzoic acid 1-isopropyl-benzo[def]chrysen-8-yl ester (107616-92-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.2 g / p-toluenesulfonic acid / benzene / 24 h / Heating

2: 50 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 0.5 h / Heating

With toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene;

DOI:10.1021/jo00387a023

Downstream raw materials:

Benzoic acid 1-isopropyl-9,10-dihydro-benzo[def]chrysen-8-yl ester

Benzoic acid 1-isopropyl-benzo[def]chrysen-8-yl ester

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