[RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF₆

Base Information

• Chemical Name: [RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF₆
• CAS No.: 1174750-01-6
• Molecular Formula: C₃₂H₃₈ClN₂RuS₂*F₆P
• Molecular Weight: 796.286

Synonyms:[RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF₆

Chemical Property of [RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF₆

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Technology Process of [RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF₆

There total 1 articles about [RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

potassium hexafluorophosphate (17084-13-8) + [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + 1,3-bis(2,4,6-trimethylphenyl)imidazolium-2-dithiocarboxylate (917604-43-4) → [RuCl(4-isopropyltoluene)(1,3-di(2,4,6-trimethylphenyl)-imidazolium-2-dithiocarboxylate)]PF6 (1174750-01-6)

Guidance literature:

In ethanol; byproducts: KCl; under Ar; EtOH added to mixt. of Ru complex, dithiocarboxylate and KPF6;heated at 60°C (oil bath) for 1 h under normal atm. pressure; co oled to room temp.; volatiles evapd. under vac.; taken up with CH2Cl2; filtered (Celite); rised with CH2Cl2; filtrate evapd. on rotary evaporator; recrystd. from CHCl3-cyclohexane; dried under high vac.; elem. anal.;

DOI:10.1021/om9002363

upstream raw materials:

potassium hexafluorophosphate

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

1,3-bis(2,4,6-trimethylphenyl)imidazolium-2-dithiocarboxylate

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