N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

Base Information

Chemical Name:N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide
CAS No.:155447-66-8
Molecular Formula:C₁₄H₉F₃N₂O
Molecular Weight:278.233
Hs Code.:

N<sup>1</sup>-(4-oxo-2,5-cyclohexadien-1-ylidene)-N<sup>2</sup>-phenyl-2,2,2-trifluoroethanimidamide

Synonyms:N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

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Chemical Property of N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

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Technology Process of N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

There total 4 articles about N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 155447-39-5
N-(4-methoxyphenyl)-N'-phenyl-2,2,2-trifluoroethanimidamide

: 155447-66-8
N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

Guidance literature:: With water; In acetonitrile; at -10 ℃; electrolysis: NaClO₄, glassy carbon anode, platinum foil cathode; 5 mA/cm² for 2.5-3.0 F/mol;
DOI:10.1021/jo00090a017

Reference yield: 13.0%

: 155447-39-5
N-(4-methoxyphenyl)-N'-phenyl-2,2,2-trifluoroethanimidamide

: 155447-66-8
N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

: 1-(4-methoxyphenyl)-2-(trifluoromethyl)-1H-benzo[d]imidazole

: 1-phenyl-2-(trifluoromethyl)-6-methoxybenzimidazole

Guidance literature:: In acetonitrile; at 60 ℃; electrolysis: NaClO₄, glassy carbon anode, platinum foil cathode; 5 mA/cm² for 2.1 F/mol;
DOI:10.1021/jo00090a017

Reference yield:

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 155447-66-8
N¹-(4-oxo-2,5-cyclohexadien-1-ylidene)-N²-phenyl-2,2,2-trifluoroethanimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaH / tetrahydrofuran / 0.5 h / 68 °C

2: 91 percent / H₂O / acetonitrile / -10 °C / electrolysis: NaClO₄, glassy carbon anode, platinum foil cathode; 5 mA/cm² for 2.5-3.0 F/mol

With water; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00090a017