N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

Base Information

Chemical Name:N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide
CAS No.:940290-17-5
Molecular Formula:C₂₄H₂₅N₃O₄
Molecular Weight:419.48
Hs Code.:

Synonyms:N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

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Chemical Property of N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

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Technology Process of N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

There total 3 articles about N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61-54-1
tryptamine

: 940290-17-5
N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 78 percent / tetrahydrofuran / 20 °C

2.1: 98 percent / H₂ / Pd/C / methanol / 1 h / 20 °C

3.1: Et₃N; ethyl chloroformate / tetrahydrofuran / 1 h / 0 °C

3.2: 47 percent / Et₃N / tetrahydrofuran / 20 °C

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2007.02.023

Reference yield:

: 145118-42-9
N²-(benzyloxycarbonyl)-N¹-<2-(1H-indol-3-yl)ethyl>alaninamid

: 940290-17-5
N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / H₂ / Pd/C / methanol / 1 h / 20 °C

2.1: Et₃N; ethyl chloroformate / tetrahydrofuran / 1 h / 0 °C

2.2: 47 percent / Et₃N / tetrahydrofuran / 20 °C

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2007.02.023

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 940290-17-5
N-(3-(4-acetoxyphenyl)-propenoyl)-L-alanine tryptamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 86 percent / pyridine / 20 °C

2.1: Et₃N; ethyl chloroformate / tetrahydrofuran / 1 h / 0 °C

2.2: 47 percent / Et₃N / tetrahydrofuran / 20 °C

With pyridine; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2007.02.023