diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

Base Information

Chemical Name:diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate
CAS No.:126865-13-2
Molecular Formula:C₂₁H₂₅F₃O₆S₂
Molecular Weight:494.553
Hs Code.:

Synonyms:diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

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Technology Process of diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

There total 1 articles about diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 20461-99-8
ethyl 1,3-dithiolane-2-carboxylate

: 52505-37-0
2'-trifluoromethylbenzylidenemalonic acid diethyl ester

: 126865-13-2
diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h;
DOI:10.1002/jhet.5570260525

Reference yield:

: 126865-13-2
diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

: 126884-28-4
2-Ethoxycarbonyl-4-oxo-3-(2-trifluoromethyl-phenyl)-pentanedioic acid diethyl ester

Guidance literature:: With N-Bromosuccinimide; In water; acetonitrile; at 0 ℃; for 0.5h;
DOI:10.1002/jhet.5570260525

Reference yield:

: 126865-13-2
diethyl <2-(ethoxycarbonyl-1,3-dithiolan-2-yl)<2-(trifluoromethyl)phenyl>methyl>propanedioate

: 126865-15-4
trans-diethyl 1,4,5,6-tetrahydro-6-oxo-4-<2-(trifluoromethyl)phenyl>-3,5-pyridazinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 3.7 g / N-bromosuccinimide / acetonitrile; H₂O / 0.5 h / 0 °C

2: 1.) anhydrous hydrazine, 2.)toluenesulfonic acid hydrate / 1.) ethanol, room temperature, overnight, 2.) reflux, 4 h

With N-Bromosuccinimide; toluene-4-sulfonic acid; hydrazine; In water; acetonitrile;
DOI:10.1002/jhet.5570260525