Technology Process of C24H23N3O5
There total 3 articles about C24H23N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide; triethylamine; trifluoroacetic acid;
In
acetonitrile;
for 4h;
Ambient temperature;
DOI:10.1021/jm9606094
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 76 percent / MeONa, MeOH / 3 h / Ambient temperature
2: 1.) NaH / 1.) DMF, -50 deg C, 2 h, 2.) DMF, -50 deg C, 2 h
3: 49 percent / 1.) HBr, TFA, 2.) Et3N / acetonitrile / 4 h / Ambient temperature
With
methanol; hydrogen bromide; sodium methylate; sodium hydride; triethylamine; trifluoroacetic acid;
In
acetonitrile;
DOI:10.1021/jm9606094
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) NaH / 1.) DMF, -50 deg C, 2 h, 2.) DMF, -50 deg C, 2 h
2: 49 percent / 1.) HBr, TFA, 2.) Et3N / acetonitrile / 4 h / Ambient temperature
With
hydrogen bromide; sodium hydride; triethylamine; trifluoroacetic acid;
In
acetonitrile;
DOI:10.1021/jm9606094