N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide

Base Information

Chemical Name:N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide
CAS No.:125159-86-6
Molecular Formula:C₁₈H₂₀Cl₄N₂O₂S
Molecular Weight:470.247
Hs Code.:

Synonyms:N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide

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Technology Process of N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide

There total 2 articles about N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.3%

: 125159-88-8
N-methyl-4,5-pentamethylenepyrrole

: 81924-15-4
N-(2,2,2-trichloroethylidene)-4-chlorobenzenesulfonamide

: 125159-86-6
N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide

Guidance literature:: With boron trifluoride diethyl etherate; In benzene; at 40 - 45 ℃; for 4h;

Reference yield:

: 17260-65-0
N,N-dichloro-4-chlorobenzenesulfonamide

: 125159-86-6
N-<2,2,2-trichloro-1-(1-methyl-4,5-pentamethylene-2-pyrrolyl)ethyl>-p-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 9 h / 87 °C

2: 52.3 percent / boron trifluoride etherate / benzene / 4 h / 40 - 45 °C

With boron trifluoride diethyl etherate; In benzene;