2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose

Base Information

• Chemical Name: 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose
• CAS No.: 193695-22-6
• Molecular Formula: C₆₀H₄₈O₁₇
• Molecular Weight: 1041.03

Synonyms:2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose

Chemical Property of 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose

Chemical Property:

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Technology Process of 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose

There total 1 articles about 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,2,3,4-tetra-O-benzoyl-α-D-glucopyranose (114298-48-5) + 2,3,4-tri-O-benzoyl-α-D-xylopyranosyl bromide (14262-83-0) → C60H48O17 + 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose (193695-22-6)

Guidance literature:

With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -20 ℃; for 42h;

DOI:10.1016/S0008-6215(97)00086-4

Reference yield: 28.0%

2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose (193695-22-6) → 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranose

Guidance literature:

With hydrazinium monoacetate; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

DOI:10.1016/S0008-6215(97)00086-4

Reference yield:

2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-α-D-glucopyranose (193695-22-6) → 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranosyl bromide (192827-11-5)

Guidance literature:

With hydrogen bromide; acetic acid; In dichloromethane; at 15 ℃; for 4h;

DOI:10.1016/S0008-6215(97)00086-4

upstream raw materials:

1,2,3,4-tetra-O-benzoyl-α-D-glucopyranose

2,3,4-tri-O-benzoyl-α-D-xylopyranosyl bromide

Downstream raw materials:

2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-glucopyranosyl bromide

linaloyl 2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranoside

(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside

(3R)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside

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