C₅₃H₇₃N₇O₁₃

Base Information

Chemical Name:C₅₃H₇₃N₇O₁₃
CAS No.:1025935-89-0
Molecular Formula:C₅₃H₇₃N₇O₁₃
Molecular Weight:1016.2
Hs Code.:

C<sub>53</sub>H<sub>73</sub>N<sub>7</sub>O<sub>13</sub>

Synonyms:C₅₃H₇₃N₇O₁₃

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Chemical Property of C₅₃H₇₃N₇O₁₃

Chemical Property:

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Technology Process of C₅₃H₇₃N₇O₁₃

There total 13 articles about C₅₃H₇₃N₇O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3496-11-5
2,5-dioxopyrrolidin-1-yl (2S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanoate

: 1025935-89-0
C₅₃H₇₃N₇O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / N,N-diisopropylethylamine DIEA, HOBt / dimethylformamide / 0 - 20 °C

2: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

3: 78 percent / N,N'-diisopropylethylamine DIEA, HOBt / dimethylformamide / 0 - 20 °C

4: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

5: 70 percent / N-methylmorpholine hydrochloride / dimethylformamide / 4 h / -10 - 0 °C / '

6: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

7: N-methylmorpholine NMM, N,N'-dicyclohexylcarbodiimide DCC, HOBt / dimethylformamide / 1.) 0 deg C, 2 h, 2.) RT, 24 h

With 4-methyl-morpholine; hydrogen; N-methylmorpholine hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/0223-5234(92)90113-F

Reference yield:

: 6456-74-2
Glycine tert-butyl ester

: 1025935-89-0
C₅₃H₇₃N₇O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / N,N-diisopropylethylamine DIEA, HOBt / dimethylformamide / 0 - 20 °C

2: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

3: 78 percent / N,N'-diisopropylethylamine DIEA, HOBt / dimethylformamide / 0 - 20 °C

4: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

5: 70 percent / N-methylmorpholine hydrochloride / dimethylformamide / 4 h / -10 - 0 °C / '

6: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

7: N-methylmorpholine NMM, N,N'-dicyclohexylcarbodiimide DCC, HOBt / dimethylformamide / 1.) 0 deg C, 2 h, 2.) RT, 24 h

With 4-methyl-morpholine; hydrogen; N-methylmorpholine hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/0223-5234(92)90113-F

Reference yield:

: 5545-52-8
Z-D(tBu)-OH

: 1025935-89-0
C₅₃H₇₃N₇O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine NMM / dimethylformamide / 0.05 h / -10 °C

2: 70 percent / N-methylmorpholine hydrochloride / dimethylformamide / 4 h / -10 - 0 °C / '

3: H₂ / 5percent Pd/C / acetic acid; propan-2-ol / 760 Torr / Ambient temperature

4: N-methylmorpholine NMM, N,N'-dicyclohexylcarbodiimide DCC, HOBt / dimethylformamide / 1.) 0 deg C, 2 h, 2.) RT, 24 h

With 4-methyl-morpholine; hydrogen; N-methylmorpholine hydrochloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/0223-5234(92)90113-F