3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

Base Information

Chemical Name:3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester
CAS No.:140467-99-8
Molecular Formula:C₃₄H₅₄BrO₇P
Molecular Weight:685.676
Hs Code.:

Synonyms:3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

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Chemical Property of 3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

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Technology Process of 3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

There total 9 articles about 3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphorochloridic acid 3-bromomethyl-phenyl ester 3-(3-hexadecyloxy-2-methyl-phenoxy)-2-methoxy-propyl ester

: 140467-99-8
3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

Guidance literature:: With sodium acetate; In tetrahydrofuran; for 2h; Yield given;
DOI:10.1021/jm00087a023

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 140467-99-8
3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

Guidance literature:: Multi-step reaction with 8 steps

1: 33 percent / 1.) NaH, 2.) NaI / dimethylformamide; tetrahydrofuran / Ambient temperature

2: 1.) NaH, 2.) NaI / dimethylformamide; tetrahydrofuran / 18 h / 80 °C

3: aq. H₂SO₄ / methanol / 1.5 h / Heating

4: pyridine / tetrahydrofuran / 18 h

5: NaH / dimethylformamide; tetrahydrofuran / 18 h

6: Amberlyst-15 / methanol; CHCl₃ / 1.) reflux, 2.) RT, 1.5 h

7: triethylamine / CCl₄ / 17 h / Ambient temperature

8: 0.5 M aq. sodium acetate / tetrahydrofuran / 2 h

With pyridine; amberlyst-15; sulfuric acid; sodium acetate; sodium hydride; triethylamine; sodium iodide; In tetrahydrofuran; methanol; tetrachloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00087a023

Reference yield:

: 130442-06-7
3-(hexadecyloxy)-2-methylphenol

: 140467-99-8
3-(bromomethyl)phenyl 3-<3-(hexadecyloxy)-2-methylphenoxy>-2-methoxy-1-propyl phosphoric acid diester

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) NaH, 2.) NaI / dimethylformamide; tetrahydrofuran / 18 h / 80 °C

2: aq. H₂SO₄ / methanol / 1.5 h / Heating

3: pyridine / tetrahydrofuran / 18 h

4: NaH / dimethylformamide; tetrahydrofuran / 18 h

5: Amberlyst-15 / methanol; CHCl₃ / 1.) reflux, 2.) RT, 1.5 h

6: triethylamine / CCl₄ / 17 h / Ambient temperature

7: 0.5 M aq. sodium acetate / tetrahydrofuran / 2 h

With pyridine; amberlyst-15; sulfuric acid; sodium acetate; sodium hydride; triethylamine; sodium iodide; In tetrahydrofuran; methanol; tetrachloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00087a023