methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate

Base Information

Chemical Name:methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate
CAS No.:1033221-25-8
Molecular Formula:C₂₁H₂₀BrNO₃
Molecular Weight:414.299
Hs Code.:

Synonyms:methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate

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Technology Process of methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate

There total 1 articles about methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1033221-09-8
methyl-3-bromo-4-(5-ethoxy-2-formyl-5-oxopentyl)benzoate

: 100-46-9
benzylamine

: 1033221-25-8
methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate

Guidance literature:: With acetic acid; In 1,2-dichloro-ethane; for 12h; Inert atmosphere; Reflux;
DOI:10.1021/ol800330d

Reference yield: 36.0%

: 1033221-25-8
methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-3-bromobenzoate

: 1033221-79-2
methyl 4-[(1-benzyl-6-oxo-1,6-dihydropyridin-3-yl)methyl]benzoate

: 1033221-61-2
methyl 4-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]benzoate

: dimethyl 6-[(1-benzyl-6-oxo-1,6-dihydropyridin-3-yl)methyl]-6'-[(1-benzyl-6-oxo-1,4,5,6-tetrahydropyridin-3-yl)methyl]-1,1'-biphenyl-3,3'-dicarboxylate

Guidance literature:: With palladium diacetate; caesium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; at 20 - 120 ℃; Inert atmosphere;
DOI:10.1021/ol800330d