N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide

Base Information

• Chemical Name: N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide
• CAS No.: 1239955-23-7
• Molecular Formula: C₃₃H₃₆N₆O₅
• Molecular Weight: 596.686

Synonyms:N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide

Chemical Property of N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide

Chemical Property:

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Technology Process of N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide

There total 1 articles about N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-(3,3-diethoxyprop-1-ynyl)-N1,N3-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)isophthalamide (1239955-22-6) → N1,N3-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide (1239955-23-7)

Guidance literature:

5-(3,3-diethoxyprop-1-ynyl)-N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)isophthalamide; With trifluoroacetic acid; In dichloromethane; for 4h;

With sodium hydrogencarbonate; In dichloromethane;

DOI:10.1021/ja101937w

Reference yield: 42.0%

sarcosine (107-97-1,25951-24-0) + N1,N3-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)-5-(3-oxoprop-1-ynyl)isophthalamide (1239955-23-7) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → C60C2H3N(Me)CCC6H3(C(O)NHC5H3NNHC(O)CH2CMe3)2 (1239955-28-2)

Guidance literature:

In tetrahydrofuran; toluene; at 110 ℃; for 22h; Inert atmosphere; Darkness;

DOI:10.1021/ja101937w

upstream raw materials:

5-(3,3-diethoxyprop-1-ynyl)-N₁,N₃-bis(6-(3,3-dimethylbutyrylamino)pyridin-2-yl)isophthalamide

Downstream raw materials:

C₆₀C₂H₃N(Me)CCC₆H₃(C(O)NHC₅H₃NNHC(O)CH₂CMe₃)2

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