7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione

Base Information

Chemical Name:7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione
CAS No.:65341-26-6
Molecular Formula:C₂₁H₁₅NO₇
Molecular Weight:393.353
Hs Code.:

7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzo<c>phenanthridin-6,11,12(5H)-trione

Synonyms:7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione

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Chemical Property of 7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione

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Technology Process of 7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione

There total 1 articles about 7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 87960-09-6
12ξ-anilino-11,12-dihydro-11β-hydroxyoxychelerythrine

: 87960-07-4
4-formyl-7,8-dimethoxy-2-methyl-3-4',5'-methylenedioxy-2'-phenyliminomethylphenylisocarbostyril

: 65341-26-6
7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione

: 72584-79-3
12-anilinooxychelerythrine

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 1.5h; Heating;

Reference yield:

: 65341-26-6
7,8-dimethoxy-5-methyl-2,3-methylenedioxybehzophenanthridin-6,11,12(5H)-trione

: 476-33-5,70191-85-4
(+/-)-homochelidonine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) LiAlH₄ 2.) H₂, PtO₂ / 1.) THF, reflux, 4 h, 2.) EtOH, RT, 3 h

2: 99 percent / CHCl₃ / 15 h / Ambient temperature

3: CH₂Cl₂ / 1 h / Ambient temperature

4: 5percent methanolic KOH / 1 h / Heating

5: 40 percent / 10percent hydrochloric acid, 70percent HClO₄, H₂ / 40percent Pd/C / H₂O / 48 h / 50 °C

With hydrogenchloride; platinum(IV) oxide; potassium hydroxide; lithium aluminium tetrahydride; perchloric acid; hydrogen; palladium on activated charcoal; In dichloromethane; chloroform; water;