C₃₈H₅₀N₄O₅Si₂

Base Information

Chemical Name:C₃₈H₅₀N₄O₅Si₂
CAS No.:1295471-16-7
Molecular Formula:C₃₈H₅₀N₄O₅Si₂
Molecular Weight:699.01
Hs Code.:

C<sub>38</sub>H<sub>50</sub>N<sub>4</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₈H₅₀N₄O₅Si₂

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Chemical Property of C₃₈H₅₀N₄O₅Si₂

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Technology Process of C₃₈H₅₀N₄O₅Si₂

There total 12 articles about C₃₈H₅₀N₄O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₅₀F₃NO₈SSi₂

: 1295471-16-7
C₃₈H₅₀N₄O₅Si₂

Guidance literature:: With tetrabutylammoniun azide; In toluene; at 20 ℃; for 72h; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-52-1
C₃₉H₅₅NO₅Si₂

: 1295471-16-7
C₃₈H₅₀N₄O₅Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 0 °C

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

4.1: pyridine; trifluoroacetyl chloride / dichloromethane / 8 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane; water / 0 °C

6.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 1.17 h / 0 °C

7.1: pyridine / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

8.1: tetrabutylammoniun azide / toluene / 72 h / 20 °C / Molecular sieve; Inert atmosphere

With pyridine; sodium tetrahydroborate; chloro-trimethyl-silane; oxalyl dichloride; cerium(III) chloride heptahydrate; dihydrogen peroxide; tetrabutylammoniun azide; titanium tetrachloride; ozone; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; trifluoroacetyl chloride; sodium hydroxide; In methanol; dichloromethane; water; toluene; 6.1: Luche reduction;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-03-2
C₃₉H₅₃NO₅Si₂

: 1295471-16-7
C₃₈H₅₀N₄O₅Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: ozone / dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

3.1: pyridine; trifluoroacetyl chloride / dichloromethane / 8 h / 20 °C

4.1: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane; water / 0 °C

5.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 1.17 h / 0 °C

6.1: pyridine / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

7.1: tetrabutylammoniun azide / toluene / 72 h / 20 °C / Molecular sieve; Inert atmosphere

With pyridine; sodium tetrahydroborate; chloro-trimethyl-silane; cerium(III) chloride heptahydrate; dihydrogen peroxide; tetrabutylammoniun azide; titanium tetrachloride; ozone; N-ethyl-N,N-diisopropylamine; trifluoroacetyl chloride; sodium hydroxide; In methanol; dichloromethane; water; toluene; 5.1: Luche reduction;
DOI:10.1002/anie.201008079