C₃₄H₃₄N₆O₉S

Base Information

Chemical Name:C₃₄H₃₄N₆O₉S
CAS No.:1399362-72-1
Molecular Formula:C₃₄H₃₄N₆O₉S
Molecular Weight:702.745
Hs Code.:

C<sub>34</sub>H<sub>34</sub>N<sub>6</sub>O<sub>9</sub>S

Synonyms:C₃₄H₃₄N₆O₉S

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Chemical Property of C₃₄H₃₄N₆O₉S

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Technology Process of C₃₄H₃₄N₆O₉S

There total 21 articles about C₃₄H₃₄N₆O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391396-83-0
C₃₅H₃₆N₆O₉S

: 1399362-72-1
C₃₄H₃₄N₆O₉S

Guidance literature:: C₃₅H₃₆N₆O₉S; With lithium hydroxide; In methanol; dichloromethane; at 20 ℃; for 8h;

In methanol; dichloromethane; water; pH=1; Acidic conditions;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1391396-36-3
C₂₇H₃₉N₃O₈

: 1399362-72-1
C₃₄H₃₄N₆O₉S

Guidance literature:: Multi-step reaction with 14 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

4.2: 12 h / -20 - 20 °C / Inert atmosphere

5.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

5.2: pH 1 / Acidic conditions

6.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol

8.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

9.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

10.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -46 °C / Inert atmosphere

10.2: 12 h / -46 - 20 °C / Inert atmosphere

11.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

12.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

13.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

13.2: 3 h / 0 °C / Inert atmosphere

13.3: 3 h / 20 °C / Inert atmosphere

14.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

14.2: pH 1 / Acidic conditions

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 13.1: Hantzsch thiazole synthesis / 13.2: Hantzsch thiazole synthesis / 13.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1064763-79-6
Boc-L-Thr(t-Bu)-L-Ser-OMe

: 1399362-72-1
C₃₄H₃₄N₆O₉S

Guidance literature:: Multi-step reaction with 19 steps

1.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

3.2: 12 h / -20 - 20 °C / Inert atmosphere

4.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

4.2: pH 1 / Acidic conditions

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / ethanol

7.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

8.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

9.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

9.2: 12 h / -20 - 20 °C / Inert atmosphere

10.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

10.2: pH 1 / Acidic conditions

11.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

12.1: palladium 10% on activated carbon; hydrogen / ethanol

13.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

14.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

15.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -46 °C / Inert atmosphere

15.2: 12 h / -46 - 20 °C / Inert atmosphere

16.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

17.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

18.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

18.2: 3 h / 0 °C / Inert atmosphere

18.3: 3 h / 20 °C / Inert atmosphere

19.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

19.2: pH 1 / Acidic conditions

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 18.1: Hantzsch thiazole synthesis / 18.2: Hantzsch thiazole synthesis / 18.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105