Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Base Information

• Chemical Name: Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid
• CAS No.: 88772-99-0
• Molecular Formula: C₈₀H₈₃N₃O₁₄
• Molecular Weight: 1310.55

Synonyms:Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Chemical Property of Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Chemical Property:

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Technology Process of Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

There total 3 articles about Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

Phenyl-O-(2,3-di-O-benzyl-4-chlor-4,6-didesoxy-α-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (88773-01-7) → Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (88772-99-0)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; for 20h; Heating;

DOI:10.1002/jlac.198319831106

Reference yield: 22.0%

Phenyl-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (87591-19-3) + O-(4-Azido-2,3-di-O-benzyl-4,6-didesoxy-D-glucopyranosyl)-trichloracetimidat → Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid + Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (88772-99-0)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; for 4.5h; Ambient temperature;

DOI:10.1002/jlac.198319831106

Reference yield: 22.0%

Phenyl-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (87591-19-3) + trichloroacetonitrile (545-06-2) → Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid + Phenyl-O-(4-azido-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (88772-99-0)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; for 4.5h; Ambient temperature;

DOI:10.1002/jlac.198319831106

upstream raw materials:

Phenyl-O-(2,3-di-O-benzyl-4-chlor-4,6-didesoxy-α-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Phenyl-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

trichloroacetonitrile

Downstream raw materials:

Phenyl-O-(4-amino-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(α-D-glucopyranosyl)-(1->4)-α-D-glucopyranosid

Phenyl-O-(4-amino-2,3-di-O-benzyl-4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

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