1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

Base Information

Chemical Name:1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene
CAS No.:1228259-76-4
Molecular Formula:C₂₀H₁₂BrF₁₇
Molecular Weight:655.192
Hs Code.:

Synonyms:1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

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Chemical Property of 1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

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Technology Process of 1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

There total 2 articles about 1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 107-19-7
propargyl alcohol

: 1228259-73-1
9,9,10,10,11,11,12,12,13,13,14,14,14-tridecafluorotetradec-1-yne

: 1228259-74-2
9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadec-1-yne

: 1228259-72-0
7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-yne

: C₁₄H₂₁BrO₂Si₂

: 173019-84-6
1-bromo-4-(3-bromoprop-1-yn-1-yl)benzene

: 1228259-78-6
1-bromo-4-(9,9,10,10,11,11,12,12,13,13,14,14,14-tridecafluorotetradec-1-ynyl)benzene

: 1228259-79-7
1-bromo-4-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadec-1-ynyl)benzene

: 912663-67-3
(Z)-2-[2-(4-bromophenyl)-3-phenyl-1H-inden-1-ylidene]propanal

: 1228259-76-4
1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / 80 °C

2: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C / Inert atmosphere

With potassium carbonate; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; In tetrahydrofuran; water; toluene;

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 107-19-7
propargyl alcohol

: 1228259-73-1
9,9,10,10,11,11,12,12,13,13,14,14,14-tridecafluorotetradec-1-yne

: 1228259-74-2
9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadec-1-yne

: 1228259-72-0
7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-yne

: C₁₄H₂₁BrO₂Si₂

: 173019-84-6
1-bromo-4-(3-bromoprop-1-yn-1-yl)benzene

: 1228259-78-6
1-bromo-4-(9,9,10,10,11,11,12,12,13,13,14,14,14-tridecafluorotetradec-1-ynyl)benzene

: 1228259-79-7
1-bromo-4-(9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,16,16-heptadecafluorohexadec-1-ynyl)benzene

: 912663-67-3
(Z)-2-[2-(4-bromophenyl)-3-phenyl-1H-inden-1-ylidene]propanal

: 1228259-76-4
1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

: (E)-2-[2-(4-bromophenyl)-3-phenyl-1H-inden-1-ylidene]propanal

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / 80 °C

2: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C / Inert atmosphere

With potassium carbonate; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; In tetrahydrofuran; water; toluene;

Reference yield: 99.0%

: 1228259-76-4
1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradec-1-ynyl)benzene

: 1228259-60-6
1-bromo-4-(7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptadecafluorotetradecyl)benzene

Guidance literature:: With 5% rhodium-on-charcoal; hydrogen; In dichloromethane; pentane; at 20 ℃; under 37503.8 Torr; Autoclave;
DOI:10.1055/s-0029-1218667