Technology Process of C23H27BrN4O2
There total 5 articles about C23H27BrN4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tert-butyl alcohol
2: sodium periodate; silica gel / dichloromethane
3: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
5: trifluoroacetic acid / dichloromethane
With
sodium chlorite; sodium periodate; osmium(VIII) oxide; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; silica gel; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.03.112
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium periodate; silica gel / dichloromethane
2: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
4: trifluoroacetic acid / dichloromethane
With
sodium chlorite; sodium periodate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; silica gel; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.03.112