2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine

Base Information

Chemical Name:2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine
CAS No.:89129-04-4
Molecular Formula:C₂₃H₂₉N₃O₈
Molecular Weight:475.499
Hs Code.:

Synonyms:2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine

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Chemical Property of 2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine

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Technology Process of 2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine

There total 1 articles about 2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 53386-64-4
methyl 2-(benzylamino)acetate

: 89148-09-4
5-chloromethyluridine

: 89129-04-4
2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1016/S0040-4039(00)87878-8

Reference yield:

: 89129-04-4
2',3'-O-isopropylidene-5-<(N-benzyl)methoxycarbonylmethylaminomethyl>uridine

: 69181-26-6
5-carboxymethylaminomethyluridine

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10percent Pd/C / methanol / 5 h / 25 °C / 760 Torr

2: pyridine / 12 h / Ambient temperature

3: 80 percent / 5percent NaHCO₃ / H₂O

4: 50percent acetic acid / 0.75 h / 100 °C

5: Ba(OH)2 / H₂O

With barium dihydroxide; hydrogen; sodium hydrogencarbonate; acetic acid; palladium on activated charcoal; In pyridine; methanol; water;
DOI:10.1016/S0040-4039(00)87878-8