3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

Base Information

Chemical Name:3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol
CAS No.:915948-83-3
Molecular Formula:C₁₆H₁₇N₃O₃
Molecular Weight:299.329
Hs Code.:

Synonyms:3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

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Chemical Property of 3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

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Technology Process of 3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

There total 6 articles about 3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-{3-(benzyloxy)-5-[(1S)-2-methoxy-1-methylethoxy]phenyl}-3H-imidazo[4,5-b]pyridine

: 915948-83-3
3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; ethyl acetate; for 16h;

Reference yield:

: 851885-41-1
3-{[(1S)-1-methyl-2-(methyloxy)ethyl]oxy}-5-[(phenylmethyl)oxy]benzoic acid

: 915948-83-3
3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

Guidance literature:: Multi-step reaction with 3 steps

1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 2 h

2: acetic acid / xylene / 4.5 h / 140 - 150 °C

3: hydrogen / palladium 10% on activated carbon / methanol; ethyl acetate / 16 h

With hydrogen; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium 10% on activated carbon; In methanol; ethyl acetate; N,N-dimethyl-formamide; xylene;

Reference yield:

: 851885-42-2
methyl 3-{[(1S)-1-methyl-2-(methyloxy)ethyl]oxy}-5-[(phenylmethyl)oxy]benzoate

: 915948-83-3
3-(3H-imidazo[4,5-b]pyridin-2-yl)-5-[(1S)-2-methoxy-1-methylethoxy]phenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; sodium hydroxide / tetrahydrofuran / 4 h / 20 °C

1.2: pH 4

2.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 2 h

3.1: acetic acid / xylene / 4.5 h / 140 - 150 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol; ethyl acetate / 16 h

With methanol; sodium hydroxide; hydrogen; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; xylene;