C₂₃H₁₉NO

Base Information

Chemical Name:C₂₃H₁₉NO
CAS No.:1383563-76-5
Molecular Formula:C₂₃H₁₉NO
Molecular Weight:325.41
Hs Code.:

Synonyms:C₂₃H₁₉NO

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Chemical Property of C₂₃H₁₉NO

Chemical Property:

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Technology Process of C₂₃H₁₉NO

There total 4 articles about C₂₃H₁₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1301262-42-9
C₁₇H₁₃NO₂

: 1383563-76-5
C₂₃H₁₉NO

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C / 760.05 Torr

2: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; potassium hexamethylsilazane; sodium carbonate; In tetrahydrofuran; ethanol; water; toluene; 3: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290504

Reference yield:

: 137643-61-9
C₁₇H₁₅NO₂

: 1383563-76-5
C₂₃H₁₉NO

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium hexamethylsilazane; sodium carbonate; In tetrahydrofuran; water; toluene; 2: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290504

Reference yield:

: 35299-03-7
N-benzyl-2-vinylbenzamide

: 1383563-76-5
C₂₃H₁₉NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 5 h / -78 - 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 5 h / Reflux

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C / 760.05 Torr

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; potassium hexamethylsilazane; sodium hydride; sodium carbonate; In tetrahydrofuran; ethanol; water; toluene; 5.1: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290504