C₂₇H₂₂BNO₂

Base Information

Chemical Name:C₂₇H₂₂BNO₂
CAS No.:1369587-64-3
Molecular Formula:C₂₇H₂₂BNO₂
Molecular Weight:403.288
Hs Code.:

C<sub>27</sub>H<sub>22</sub>BNO<sub>2</sub>

Synonyms:C₂₇H₂₂BNO₂

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Chemical Property of C₂₇H₂₂BNO₂

Chemical Property:

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Technology Process of C₂₇H₂₂BNO₂

There total 5 articles about C₂₇H₂₂BNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1369587-63-2
10-(3-bromophenyl)-12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 1369587-64-3
C₂₇H₂₂BNO₂

Guidance literature:: 10-(3-bromophenyl)-12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

With Triisopropyl borate; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

With ammonium chloride; In tetrahydrofuran; hexane; water;

Reference yield:

: 95-51-2
o-chloroaniline

: 1369587-64-3
C₂₇H₂₂BNO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 9 h / 120 °C

2.1: sodium carbonate / palladium diacetate; tricyclohexylphosphine tetrafluoroborate / ISOPROPYLAMIDE / 3 h / 190 °C

3.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 24 h / 120 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

4.2: 2 h / -78 °C

With n-butyllithium; sodium carbonate; sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate; tricyclohexylphosphine tetrafluoroborate; In tetrahydrofuran; hexane; ISOPROPYLAMIDE; toluene;

Reference yield:

: 28320-31-2
2-bromo-9,9-dimethyl-9H-fluorene

: 1369587-64-3
C₂₇H₂₂BNO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 9 h / 120 °C

2.1: sodium carbonate / palladium diacetate; tricyclohexylphosphine tetrafluoroborate / ISOPROPYLAMIDE / 3 h / 190 °C

3.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 24 h / 120 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

4.2: 2 h / -78 °C

With n-butyllithium; sodium carbonate; sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate; tricyclohexylphosphine tetrafluoroborate; In tetrahydrofuran; hexane; ISOPROPYLAMIDE; toluene;