1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

Base Information

Chemical Name:1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane
CAS No.:57430-12-3
Molecular Formula:C₁₈H₂₀O₅
Molecular Weight:316.354
Hs Code.:

Synonyms:1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

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Chemical Property of 1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

Chemical Property:

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Technology Process of 1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

There total 4 articles about 1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 122767-87-7
3',5'-dimethyl-4,5-methylenedioxy-2,2',4'-trihydroxydihydrochalcone

: 57430-12-3
1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

Guidance literature:: With hydrogenchloride; amalgamated zinc; In ethanol; for 0.5h; Heating;
DOI:10.1016/0031-9422(89)85046-0

Reference yield:

: 19202-31-4
6-(benzyloxy)benzo[d][1,3]dioxole-5-carbaldehyde

: 57430-12-3
1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent

2: 75 percent / H₂ / 10percent Pd-C / ethanol; CHCl₃; acetic acid / 4.5 h / 2585.7 Torr

3: 66 percent / amalgamated Zn, cc. HCL / aq. ethanol / 0.5 h / Heating

With hydrogenchloride; amalgamated zinc; hydrogen; palladium on activated charcoal; In ethanol; chloroform; acetic acid;
DOI:10.1016/0031-9422(89)85046-0

Reference yield:

: 1-(2,4-Bis-benzyloxy-3,5-dimethyl-phenyl)-ethanone

: 57430-12-3
1-(2',4'-dihydroxy-3',5'-dimethylphenyl)-3-(2-hydroxy-4,5-methylenedioxyphenyl)-propane

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent

2: 75 percent / H₂ / 10percent Pd-C / ethanol; CHCl₃; acetic acid / 4.5 h / 2585.7 Torr

3: 66 percent / amalgamated Zn, cc. HCL / aq. ethanol / 0.5 h / Heating

With hydrogenchloride; amalgamated zinc; hydrogen; palladium on activated charcoal; In ethanol; chloroform; acetic acid;
DOI:10.1016/0031-9422(89)85046-0