(3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

Base Information

Chemical Name:(3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate
CAS No.:1365542-98-8
Molecular Formula:C₁₆H₂₈O₆
Molecular Weight:316.395
Hs Code.:

Synonyms:(3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

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Chemical Property of (3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

Chemical Property:

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Technology Process of (3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

There total 3 articles about (3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-22-0
pentan-3-one

: 1365542-98-8
(3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: orthoformic acid triethyl ester

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 40 °C

3: triethylsilane; titanium tetrachloride / dichloromethane / -78 - -10 °C

With triethylsilane; dmap; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; orthoformic acid triethyl ester; In dichloromethane;
DOI:10.1016/j.tetlet.2012.01.017

Reference yield:

: 138-59-0
shikimic acid

: 1365542-98-8
(3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: benzenesulfonic acid

2: orthoformic acid triethyl ester

3: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 40 °C

4: triethylsilane; titanium tetrachloride / dichloromethane / -78 - -10 °C

With triethylsilane; dmap; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; orthoformic acid triethyl ester; benzenesulfonic acid; In dichloromethane;
DOI:10.1016/j.tetlet.2012.01.017

Reference yield:

: 101769-63-5
(3R,4S,5R)-3,4,5-trihydroxycyclohex-1-ene-1-carboxylic acid ethyl ester

: 1365542-98-8
(3R,4S,5R)-ethyl 4-hydroxy-5-(methoxymethoxy)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: orthoformic acid triethyl ester

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 40 °C

3: triethylsilane; titanium tetrachloride / dichloromethane / -78 - -10 °C

With triethylsilane; dmap; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; orthoformic acid triethyl ester; In dichloromethane;
DOI:10.1016/j.tetlet.2012.01.017