((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

Base Information

Chemical Name:((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester
CAS No.:913180-60-6
Molecular Formula:C₁₃H₁₉NO₅S
Molecular Weight:301.364
Hs Code.:

Synonyms:((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

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Chemical Property of ((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

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Technology Process of ((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

There total 2 articles about ((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: C₅H₁₃NO₃S

: 913180-60-6
((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2006.07.033

Reference yield:

: (S)-2-Benzyloxycarbonylamino-4-methanesulfonyl-butyric acid

: 913180-60-6
((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

Guidance literature:: (S)-2-Benzyloxycarbonylamino-4-methanesulfonyl-butyric acid; With triethylamine; isobutyl chloroformate; In tetrahydrofuran;

With sodium tetrahydroborate; In water;
DOI:10.1016/j.bmcl.2005.12.095

Reference yield:

: 913180-60-6
((S)-1-Hydroxymethyl-3-methanesulfonyl-propyl)-carbamic acid benzyl ester

: 913180-85-5
4-methanesulfonyl-N¹-(4-trifluoromethoxy-phenyl)-butane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodinane / CH₂Cl₂

2: NaB(CN)H₃; AcOH / methanol

3: H₂ / Pd/C / ethanol

With hydrogen; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.07.033