Technology Process of 5-deaza-10-formyl-5,6,7,8-tetrahydropteroic acid
There total 5 articles about 5-deaza-10-formyl-5,6,7,8-tetrahydropteroic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; trifluoroacetic acid;
platinum(IV) oxide;
at 25 ℃;
for 3h;
under 2327.2 - 2844.3 Torr;
DOI:10.1021/jm00089a009
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) glacial AcOH, 2.) 3-Angstroem molecular sieves, 3.) (CH3)3CNH2*BH3
2: 86 percent / 0.5 N NaOH / 8 h / Heating
3: 79 percent / Ac2O / 3 h / Ambient temperature
4: 76 percent / H2, CF3COOH / PtO2 / 3 h / 25 °C / 2327.2 - 2844.3 Torr
With
sodium hydroxide; 3 A molecular sieve; N-tert-butylaminoborane; hydrogen; acetic anhydride; acetic acid; trifluoroacetic acid;
platinum(IV) oxide;
DOI:10.1021/jm00089a009
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) glacial AcOH, 2.) 3-Angstroem molecular sieves, 3.) (CH3)3CNH2*BH3
2: 86 percent / 0.5 N NaOH / 8 h / Heating
3: 79 percent / Ac2O / 3 h / Ambient temperature
4: 76 percent / H2, CF3COOH / PtO2 / 3 h / 25 °C / 2327.2 - 2844.3 Torr
With
sodium hydroxide; 3 A molecular sieve; N-tert-butylaminoborane; hydrogen; acetic anhydride; acetic acid; trifluoroacetic acid;
platinum(IV) oxide;
DOI:10.1021/jm00089a009
