Technology Process of C28H26N4O6S
There total 5 articles about C28H26N4O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
at 20 ℃;
for 10h;
DOI:10.1038/nchem.1796
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; C64H45F6NP(1+)*I(1-) / toluene / 0 °C
2.1: ozone / dichloromethane / 0.17 h / -78 °C
2.2: 2 h / -78 - 20 °C
3.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -78 °C
3.2: 7 h / 20 °C
4.1: acetonitrile / 6 h / Reflux
5.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 10 h / 20 °C
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; C64H45F6NP(1+)*I(1-); diisobutylaluminium hydride; ozone; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane; toluene; acetonitrile;
5.1: |Mitsunobu Displacement;
DOI:10.1038/nchem.1796
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ozone / dichloromethane / 0.17 h / -78 °C
1.2: 2 h / -78 - 20 °C
2.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -78 °C
2.2: 7 h / 20 °C
3.1: acetonitrile / 6 h / Reflux
4.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 10 h / 20 °C
With
diisobutylaluminium hydride; ozone; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane; acetonitrile;
4.1: |Mitsunobu Displacement;
DOI:10.1038/nchem.1796
